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Pyroligneous acid - Aldehydes and Ketones
Pyroligneous acid consisting of acetic acid, acetone and methyl alcohol that is distilled in copper vessel and the vapours are passed via hot milk of lime. Acetic acid combines to make nonvolatile calcium acetate. The methanol and acetone's unabsorbed vapours are condensed and fractionally distilled. Acetone distills at 56° C.
So the acetone obtained is purified with the help of sodium bisulphite.
Lithium aluminum hydride Lithium aluminum hydride reduces the carbonyl group to an alcohol.
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This cycloaddition reaction involves sixteen electrons; hence, it must be suprafacial on one component and antarafacial on the other. Thus, it must be a [14s + 2a] or a [14a + 2s]
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