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Radioanalytical methods:
Radioanalytical methods using radiotracers and activation analysis are more sensitive and specific because of ease of detection of nuclear radiation. Being dependent on nuclear property there is complete absence of chemical interferences. Details of isotope dilution analysis (IDA), radiometric titration, radiochromatography and radioimmunoassay including their principles of methodology, applications, advantages and limitations are discussed. The principle of neutron activation analysis, its methodology including instrumentation and typical applications are discussed. Instrumental neutron activation analysis (INAA) has the special advantage of being nondestructive and multielemental besides being blank free and hence very useful for forensic and archaeological studies. However, INAA is suited for the determination of total elemental content only but not suited for speciation studies. A comparative account of NAA and IDA with other trace analysis methods is presented. These methods are preferred in spite of the fact that specially licensed laboratory and radiation safety measures are required.
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The type of orbitals present in Fe is : (1) s (2) s and p (3) s, p and d ()s, p, d, and f Ans: s, p and d
Ring substitution in aromatic ethers Alkoxy group is ortho and para directing and it directs the incoming groups to ortho and para position. It becomes the aromatic ring leads
The maximum number of electrons which each sub-shell can occupy is: (1) 2n 2 (2) 2n (3) 2 (2l+1) (4) (2l+1) Ans: 2
The table below gives intrinsic viscosity values determined by viscometry and weight- average molar mass values determined under the same conditions by static light scattering
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The total number of unpaired electrons in d- orbital's of atoms of element of atomic number 29 is: (1) 10 (2) 1 (3) 0 (4)5 Ans: 0
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