Define procedure for estimation of iron in the solution, Science

Assignment Help:

Define Procedure for Estimation of Iron in the Solution?

Carry out the experiment following the steps enumerated herewith:

1. Weigh 702 mg of reagent grade ferrous ammonium sulphate (NH4)2Fe (SO4)2. Dissolve it in 1000 ml distilled water. Add 5 ml of conc. sulphuric acid (or 3ml of 18 M sulphuric acid). 1 ml contains 0.100 mg of ferrous iron. Warm slightly and add 5 ml concentrated potassium permanganate (KMnO4) drop by drop until it produces a permanent colour (light pink). KMnO4 is added to oxidize the ferrous to ferric. Transfer this solution to a 1 litre volumetric flask and make the volume to 1 litre mark with distilled water. This solution contains 0.1 mg iron/ml.

2. Label a series of Borosil test tubes with blank (B), standard (Sl-S6) and sample (SA 1-4) and place them in a rack.

3. Take different volumes (0.2,0.4,0.6,0.8, 1.0 and 1.2 ml) of standard solution in the labeled tubes and make the volume to 2rnl with distilled water. Add 0.5 ml conc. sulphuric acid, 1 ml potassium persulphate and 2 ml of potassium thiocyanate to all tubes. Mix. Keep for 5 minutes for colour development. Add 9.5 ml distilled water to all tubes, mix and measure the optical density at 490nm.

4. For unknown sample make up the volume upto 100 ml of the given solution. Take 0.6 ml and 0.8 ml of the solution in duplicate and proceed just as in case of standard.

5. Draw the standard curve and calculate the amount of unknown solution present.


Related Discussions:- Define procedure for estimation of iron in the solution

Fire alarms precautions for fire prevention, Fire Alarms : Most modern fir...

Fire Alarms : Most modern fire alarm systems are electric and can be activated from several points throughout a building. These points usually consist of glass-covered switches wh

Define glucose and fructose - abnormal constituents of urine, Define Glucos...

Define Glucose and Fructose - Abnormal Constituents of Urine Abnormal Constituents of Urine The detection of abnormal constituents in urine indicates the presence of certa

Atomic theory in antiquity, Atomic theory in antiquity: The oldest of  ...

Atomic theory in antiquity: The oldest of  Indian philosophical systems was Samkhya. The system envisaged that everything except consciousness evolved out of primaeval matter.

A&P, Most of the plasma is composed of?

Most of the plasma is composed of?

Describe, QUESTION (A) Describe, with diagram, the structure of a neuro...

QUESTION (A) Describe, with diagram, the structure of a neuron (B) ‘Neurons are specialized cells that carry messages.' Describe how messages are carried by neurons (C) F

To surveys a lab for its fire preparedness, TO SURVEYS A LAB FOR ITS FIRE P...

TO SURVEYS A LAB FOR ITS FIRE PREPAREDNESS As said earlier in this activity you are going to survey the labs of the institution where you are working at. Look for the fire safe

Scientific activity, Describe the factors which decide the broad area of Sc...

Describe the factors which decide the broad area of Scientific activity?

Explain the glomerulus - structures of a nephron, Explain the Glomerulus: S...

Explain the Glomerulus: Structures of a Nephron Glomerulus: It is the main filter of the nephron and lies within the Bowman's capsule. It resembles a twisted mass of tiny tubes

List the important rice products, Q. List the important rice products? ...

Q. List the important rice products? The important rice products are flaked rice, expanded rice, popped rice, instant rice, rice flour, rice starch etc.

Explain the urine creatinine test, Explain the Urine Creatinine Test Th...

Explain the Urine Creatinine Test This test measures the amount of creatinine in urine. A measurement of the serum creatinine level is often used to evaluate kidney function. U

Write Your Message!

Captcha
Free Assignment Quote

Assured A++ Grade

Get guaranteed satisfaction & time on delivery in every assignment order you paid with us! We ensure premium quality solution document along with free turntin report!

All rights reserved! Copyrights ©2019-2020 ExpertsMind IT Educational Pvt Ltd