State melted and resolidified to confirm a melting point

Reference no: EM13184766

a) Synthesized a new compound one which has never beenprepared. How would you determine its mp? What precautions couldyou take to insure that it is as accurate as possible?

b) A sample of an unknown substance, although you thinkyou know its identity. How could you establish whether or not thematerial is what you suspect?

c) Why shouldn't you use a sample that has been melted andresolidified to confirm a melting point?

d) A sample of an unknown compound has an melting point of145-154C. What conclusions would you draw? What actions would youtake?

Reference no: EM13184766

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