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1. You need to analyze a mixture of alkanes. Which separation method will you choose and why? Consider two cases: a). mixture of low molecular weight alkanes, less than 15 carbons in the molecule; b). mixture of compounds with more than 20 carbon atoms in the molecule (paraffins). 2. A solution UV transmittance is 35% at 260nm. Calculate the transmittance if you dilute 25 mL of the solution to 75.0 mL? 3. On size-exclusion chromatogram you have three peaks (2.9, 3.5, and 4.8 min). Column dead volume is 12 mL, and flow rate 4 mL/min. Are your separation conditions fit for size-exclusion requirements? Explain why. 4. 50 mL of 0.1M aqueous solution of some organic compound was brought in contact with 7 mL of octanol at 20 oC. After equilibration GC analysis of octanol phase shows component concentration of 0.4M. What is the partioning coefficient of this component? 5. Two peaks on chromatogram have retention factors k1 = 4.1 and k2 = 5.9. Column efficiency is 2000 theoretical plates, Void volume is 1 mL. Calculate the resolution between these compounds.
The temperature of a 2.25 L sample of gas decreases from 35C to 20C. What is the new volume?
If 2 x 10-4 moles of S2O82- in 50 mL solution are consumed in 188 seconds, what is the rate of consumption of S2O82-
Write and equation for the reaction of Ba+ with CrO4 2-. Using the eqution you have written, explain how the addition of HCl shifts the equilibrium of the reaction
What would the product be in an aldol condensation and dehydration reaction for 4-methoxybenzaldehyde
identify the following as elements or compounds a nh3 b n2 c co d co and e he. give the numbers of protons and
A researcher studyng the nutritional value of a new candy places a 4.50 gram sample of the candy inside a bomb calorimeter and combusts it in excess oxygen
Calculate the maximum concentration of fluoride ion that could be present in hard water. Assume the only anion present that will precipitate is the calcium ion. (CaF2(s) Ksp,25C=4.0x10^-11)
Given stock solutions of 3 M Potassium Acetate and 500 mM EDTA, and a jar of solid Tris powder (molecular mass = 121 g/mol), how much of each component (including water) do you need to make 200 mL of a solution of 75 mM Potassium Acetate, 20 mM ED..
H3PO4 behaves differently at different higher temperatures, give details of reaction that occurs at different temperatures
A 55.0-{ g} piece of ice at 0.0 C is added to a sample of water at 8.0 C. All of the ice melts and the temperature of the water decreases to 0.0 C.
When performing your experiment, you add your first drop of oleic acid/benzene solution, and a lens forms immediately. What is wrong with your setup
at a particular temperature k 3.75 for the following reaction.so2g no2g so3g nogif all four gases had initial
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