The Aldol-Tishchenko reaction is a tandem reaction including an Aldol reaction and a Tishchenko reaction. In organic synthesis it is a process to change aldehydes and ketones into 1,3-hydroxyl compounds. The reaction series in various examples starts from conversion of a ketone into an enolate by action of Lithium diisopropylamide (LDA). The mono-ester diol is then changed into the diol by a hydrolysis step. With both the propiophenone and acetyl trimethylsilane as reactants, the diol is achieved as a pure diastereoisomer.
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